Kilo Lab systems
Products Range
Universal Reaction/Distillation unit
Reactor Options
- Glass
- Glass lined
- Hastalloy
- SS
- Triple Wall Glass Reactor
Operating Conditions
- Temperature
- (–90°C) up to 220°C
- Pressure
- Glass Triple Wall Reactor /Glass reactor (Full vacuum up to 0.5 bar)
- SS, Hastlloy and Glass Lined reactor (Full vacuum up to 0.6 bar)
- special Design up to 20 bar
- Capacities
- 10 L up to 500 L
- Salient Features
- CGMP design
- Instrumentation & Control
- Automation with Data Acquisition
- Skid Mounted
- Documentation
Reactor Bottom Pan
- Triple wall reactors upto 100L. Both ends fused triple wall (vacuum jacketed) glass reactor
- Glass lined
- (20L, 50L, 100L, 250L)
- Pre-insulated (with SS cladding)
- jacketed
- Cylindrical Jacketed Glass (Double Wall) up to 50L
- SS, Hastalloy, Pre-insulated Jacketed
Reactor Top Cover
- Glass top cover
- Glass lined, SS, Hastalloy for pressure reactions (standard up to 6 bar, special design up to 20 bar)
Stirrer System
- Glass lined
- Anchor
- Pitch Blade turbine curved blade turbine
- PTFE lined
- Anchor
- PBT
- Paddle,etc-multistage & interchangeable impellers also available Possibl
- Glass
- Anchor
- Turbine
- Suction agitators
- Motor
- Ex-proof
- Speed control by VFD or mechanical variator
- Suitable gear box
- Seal
- Suitable MOC
- Complete SS construction (option). SS hood for motor, gearbox, housing (standard)
Bottom Outlet Valve
- Flush with zero dead volume
- Glass / PTFE
- Glass lined with temperature sensor (optional)
Reactor Bottom Pan – Raising / Lowering Device
- Manual or motorized
- Also removable after lowering
Safety Devices
- Glass / PTFE Pressure Relief Valve
- Rupture Disc
- Translucent coating of glass components
Support Structure
- Complete SS construction
- Special designs for low headrooms
- Suitable for installation in walk-in fume hoods
- Skid mounted mobile units also possible
Flanges
- Special design high strength re-enforced plastic as standard.
- SS also available as option
- SS nut bolts with compression springs as standard.
- PTFE coated as option.
Online Sampling
- Continuous on-line liquid sampling from the reactor
Single Fluid Heating Cooling Units
- Compact unit for both heating As well as cooling
- Advanced automation to precisely control temperature
- Temperature range: -90°C up to 220°C
- Fully transparent allowing clear vision of process
- Minimum time to reach desired temperature
- Compact unit
Solid Handling Systems
- Jet Mill Micronizer, Double Cone Vacuum Dryer, and Tray Dryer, Vibro-Sifters, Cream ointment & Planetary Mixer, Tripple Roll Mill / Ball Mill, Colloid Mill, Multimill
Mobile Glass Nutsche Filters
- Suitable for acidic media filtrations
- Vacuum is used to speed up filtration
- Filter plate is made of PTFE / GF
- PTFE cloth used for filter tissue
- Mounted on wheels
Mobile Gas Scrubbers
- Simple in design
- Suitable for air & Exhaust clean up tasks
- Ideal for scrubbing exhaust From small scale chemical plants
- Ideal for studies & scale-up of gas scrubber systems
Specifications
| DESCRIPTION | JE-KL-10 | JE-KL-20 | JE-KL-30 | JE-KL-50 | JE-KL-100 | JE-KL-200 | REMARKS / DETAILED DESCRIPTION |
|---|---|---|---|---|---|---|---|
| GLASS MAIN PARTS | |||||||
| Glass Cylindrical Reactor | 10L | 20L | 30L | 50L | 100L | 200L | Option available for Jacketed and Triple Wall (vacuum jacketed) available only upto 100L reactor. L/D ratio of the reactor to be maintained. |
| Top dish |
N1: DN40 (center nozzle) N2: DN25 (side nozzle) N3: DN25 (side nozzle) N4: DN50 (front nozzle) N5: DN50 (side nozzle) N6: DN15 (side nozzle) |
N1: DN50 (center nozzle) N2: DN25 (side nozzle) N3: DN40 (side nozzle) N4: DN80 (front nozzle) N5: DN80 (side nozzle) N6: DN25 (side nozzle) |
N1: DN50 (center nozzle) N2: DN25 (side nozzle) N3: DN40 (side nozzle) N4: DN100 (front nozzle) N5: DN100 (side nozzle) N6: DN25 (side nozzle) |
Option for SS-PFA lined top dish also available. Nozzle schedule can be modified based on the customer’s requirements. | |||
| SS-PTFE Lined Agitator | 1 | 1 | 1 | 1 | 1 | 1 | Option available for Anchor, PBT, CBT impeller in single as well as dual stage. Proper L/D ratio shall be maintained. |
| Drive assembly for agitator | 0.25 HP | 0.25 HP | 0.5 HP | 0.5 HP | 1 HP | 1 HP | Flameproof motor (option available for ATEX certified), gearbox, single mechanical. |
| Glass Feed Vessel | 2L | 5L | 10L | 10L | 20L | 20L | Options available in cylindrical as well as spherical vessel, also option available for twin vessels.Vessels to be graduated and calibrated. |
| Glass Receiver Vessel | 5L | 5L | 10L | 10L | 20L | 20L | Options available in cylindrical as well as spherical vessel, also option available for twin vessels as well as single vessel. Vessels to be graduated and calibrated. |
| Glass Vapour Line | DN40 | DN50 | DN80 | DN80 | DN100 | DN150 | Option available for packing inside the column – structured (eg. Ceramic) or unstructed (eg. Glass Raschig rings) packing. |
| Glass Primary Condenser | DN80-C; 0.3 sq.m | DN80-C; 0.3 sq.m | DN100-C; 0.5 sq.m | DN150-C; 1 sq.m | DN150-C; 3 sq.m | DN225-C; 6 sq.m | S – Shell & Tube Type C – Coil Type (Options available for shell & tube type as primary condenser from 50L onwards) |
| Glass Secondary Condenser | DN80-C; 0.3 sq.m | DN80-C; 0.3 sq.m | DN80-C; 0.3 sq.m | DN80-C; 0.3 sq.m | DN100-C; 0.5 sq.m | DN100-C; 0.5 sq.m | |
| Glass Phase Separator | 1L | 2L | 2L | 2L | 2L | 2L | Dean & stark type phase separator with provision of refluxing / collecting either heavy or light phase as per the demand of the process. Option for horizontal phase separator also available. |
| Glass Vacuum Manifold | DN50 | DN50 | DN50 | DN80 | DN80 | DN80 | 5 Nozzles, drain and vent |
| Glass Ice Trap | DN80 | DN80 | DN80 | DN100 | DN100 | DN100 | For trapping the escaped vapor and preventing it from fouling the vacuum pump. Ice trap to be filled with either liquid nitrogen or dry ice. |
| Glass Internal Process Pipelines | DN15 / DN25 | DN15 / DN25 | DN15 / DN25 | DN40 / DN25 | DN40 / DN25 | DN40 / DN25 | |
| Glass Main Vacuum Line | DN25 | DN25 | DN25 | DN40 | DN40 | DN40 | |
| Glass Vacuum Balance Line to Receivers / Feed Vessels | DN15 | DN15 | DN15 | DN25 | DN25 | DN25 | |
| Hardware – Plastic flanges, Inserts , SS Nuts, bolts, washers and springs | SET | SET | SET | SET | SET | SET | Plastic flanges used as per DIN standard. Option available for SS-304 / SS-316 flanges too. |
| Structure – Main Frame – SS304 | 1″ SCH40 pipe | 1″ SCH40 pipe | 1″ SCH40 pipe | 1.25″ SCH40 pipe | 1.25″ SCH40 pipe | 1.25″ SCH40 pipe | Option available for reactor vessel lifting and lowering with limit switches. |
| SAFETY FEATURES | |||||||
| Rupture Disc | DN40 / DN50 | DN40 / DN50 | DN40 / DN50 | DN40 / DN50 | DN40 / DN50 | DN40 / DN50 | Suitable to withstand vacuum and burst pressure rating of 0.6 bar @ 100 DegC. |
| AUTOMATION AND INSTRUMENTATION | |||||||
| Temperature Sensors | 4 | 4 | 4 | 4 | 4 | 4 | Reactor temp, Vapour temp, Vent temp and Product temp. Sensor of reputed make (FLP enclosure) Duplex 3 wire Class A PT100 sensors to be used. |
| Pressure Transmitter / Dial Gauge | 1 | 1 | 1 | 1 | 1 | 1 | Please choose between pressure transmitter and dial gauge as per your requirement. |
| Agitator RPM controller (VFD) | 1 | 1 | 1 | 1 | 1 | 1 | Reputed make VFD to be used. |
| Operation & Indication Panel | 1 | 1 | 1 | 1 | 1 | 1 | Option available for: 1) Ex d enclosure (Ex II 2GD Ex DB) 2) PLC with ATEX / NON-ATEX approved HMI |
| HMI with PLC panel (Optional) | Touchscreen HMI can be provided inside flameproof enclosure along with PLC panel | Option available for: 1) Ex d enclosure (Ex II 2GD Ex DB) 2) PLC to be placed in safe area. |
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| SCADA Automation Solution (Optional) | PC workstation for controlling, storing and reviewing of process parameters of the assembly | CFR21 PART 11 compliant SCADA automation solutions, pre-defined recipe formulation as per process requirements also available. | |||||
| ADDITIONAL ACCESSORIES / INFORMATION | |||||||
| Reactor lifting and lowering system | Stainless steel lifting and lowering system for reactor vertical movement (up & down) | Used for cleaning and ease of agitator interchangeability. | |||||
| Heating & Cooling system | Different models of several temperature ranges and power (kW) are available | Do visit our product page (temperature control unit) for selection of the right model. | |||||
| Documentation (Optional) | SET | SET | SET | SET | SET | SET | Complete set of documentations and certifications to be provided along with the system. |
| Approximate Foot Print | L: 1900 mm W: 1200 mm H: 3100 mm |
L: 2000 mm W: 1000 mm H: 3300 mm |
L: 2000 mm W: 1200 mm H: 3300 mm |
L: 2150 mm W: 1300 mm H: 3300 mm |
L: 2400 mm W: 1500 mm H: 3800 mm |
L: 2650 mm W: 1500 mm H: 4200 mm |
Based on the client’s requirements, we can modify the system and try to accommodate in the available area. These footprint area is approximate, do confirm with us once. |
These are general specifications, it may deviate as per client’s requirement or at detailing stage.
